TA Instruments

AR1697-0002f

04/09/2012 15:05:19

Sample name	ASW 10 mm from base, 60 mm to top, disk 11 PMMA clean
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1697
Run number	2 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 15:05:19

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-40.78	6.058	-6.730	0.99600	22.4	102.5	2.3852	10000	0.02516	2.793	2.9815	298.15	3.384E-3	0.0	1.0	60.996	-125.10	4.847
0.9062	12.78	0.07089	1.9960	22.4	119.0	13.9290	10000	0.02922	0.7285	17.411	1741.1	3.384E-3	0.0	1.0	61.996	2.7803	10.23
1.789	19.60	0.09130	3.0120	22.4	97.54	27.5532	10000	0.02394	0.2540	34.442	3444.2	3.384E-3	0.1	1.1	63.012	5.4892	15.68
2.420	23.22	0.1042	3.9960	22.4	100.0	41.4789	10000	0.02455	0.1855	51.849	5184.9	3.383E-3	0.1	1.1	63.996	7.4238	18.58
3.901	30.97	0.1259	4.9920	22.4	103.3	68.0663	10000	0.02536	0.1077	85.083	8508.3	3.384E-3	0.1	1.1	64.992	11.967	24.78
6.089	39.58	0.1538	5.9960	22.4	111.6	107.3650	10000	0.02739	0.07123	134.21	13421	3.384E-3	0.1	1.1	65.996	18.680	31.67
6.810	42.63	0.1598	6.9960	22.4	112.4	126.9320	10000	0.02759	0.06188	158.67	15867	3.384E-3	0.1	1.1	66.996	20.894	34.10
8.684	49.21	0.1765	7.9960	22.4	106.6	165.7600	10000	0.02617	0.04404	207.20	20720	3.384E-3	0.1	1.1	67.996	26.641	39.36
11.40	57.60	0.1979	9.0000	22.4	97.54	224.0920	10000	0.02394	0.02940	280.12	28012	3.383E-3	0.2	1.2	69.000	34.971	46.08
13.14	63.75	0.2062	9.9960	22.4	96.72	275.8280	10000	0.02374	0.02380	344.79	34479	3.383E-3	0.2	1.2	69.996	40.324	51.00
15.49	69.70	0.2223	10.996	22.4	99.20	328.4740	10000	0.02435	0.02042	410.59	41059	3.383E-3	0.2	1.2	70.996	47.534	55.76
17.68	75.16	0.2353	11.996	22.4	96.72	377.9320	10000	0.02374	0.01712	472.42	47242	3.384E-3	0.2	1.2	71.996	54.248	60.12
19.54	80.54	0.2426	12.996	22.4	99.20	435.0760	10000	0.02435	0.01529	543.85	54385	3.384E-3	0.2	1.2	72.996	59.940	64.44
21.97	86.46	0.2541	13.996	22.4	84.32	498.9630	10000	0.02069	0.01128	623.70	62370	3.383E-3	0.2	1.2	73.996	67.398	69.17
25.32	94.63	0.2675	14.996	22.4	91.76	595.0270	10000	0.02252	0.01025	743.78	74378	3.384E-3	0.2	1.2	74.996	77.668	75.70
27.60	99.94	0.2761	15.996	22.4	72.75	664.7630	10000	0.01785	7.283E-3	830.95	83095	3.384E-3	0.3	1.3	75.996	84.667	79.95
30.23	105.7	0.2860	17.012	22.4	71.09	740.9780	10000	0.01745	6.365E-3	926.22	92622	3.383E-3	0.3	1.3	77.012	92.747	84.55
33.69	113.8	0.2961	18.016	22.4	68.61	855.4000	10000	0.01684	5.302E-3	1069.3	1.0693E5	3.383E-3	0.3	1.3	78.016	103.35	91.00
36.20	118.8	0.3046	18.996	22.4	57.87	931.5090	10000	0.01420	4.099E-3	1164.4	1.1644E5	3.384E-3	0.3	1.3	78.996	111.05	95.06
38.87	124.3	0.3128	20.012	22.4	62.00	1020.4600	10000	0.01522	4.015E-3	1275.6	1.2756E5	3.384E-3	0.3	1.3	80.012	119.27	99.42
42.21	132.3	0.3191	21.012	22.4	52.91	1153.7400	10000	0.01299	3.022E-3	1442.2	1.4422E5	3.384E-3	0.4	1.4	81.012	129.51	105.8
45.34	137.4	0.3300	21.996	22.4	40.51	1242.5300	10000	9.942E-3	2.146E-3	1553.2	1.5532E5	3.384E-3	0.4	1.4	81.996	139.09	109.9
47.94	142.8	0.3357	23.012	22.4	42.99	1343.9900	10000	0.01055	2.107E-3	1680.0	1.6800E5	3.384E-3	0.4	1.4	83.012	147.08	114.3
52.17	150.8	0.3459	23.996	22.4	27.28	1496.0500	10000	6.695E-3	1.199E-3	1870.1	1.8701E5	3.383E-3	0.4	1.4	83.996	160.07	120.7
54.47	155.9	0.3493	24.996	22.4	38.03	1599.5100	10000	9.333E-3	1.564E-3	1999.4	1.9994E5	3.384E-3	0.4	1.4	84.996	167.10	124.8
57.62	161.3	0.3571	25.996	22.4	17.36	1711.8400	10000	4.261E-3	6.669E-4	2139.8	2.1398E5	3.383E-3	0.4	1.4	85.996	176.78	129.1
61.97	169.3	0.3659	27.020	22.4	17.36	1882.4000	10000	4.261E-3	6.054E-4	2353.0	2.3530E5	3.384E-3	0.5	1.5	87.020	190.11	135.5
65.46	174.5	0.3752	27.996	22.4	12.40	2000.4200	10000	3.043E-3	4.074E-4	2500.5	2.5005E5	3.384E-3	0.5	1.5	87.996	200.82	139.6
68.10	179.6	0.3792	28.996	22.4	6.613	2116.4600	10000	1.623E-3	2.051E-4	2645.6	2.6456E5	3.383E-3	0.5	1.5	88.996	208.92	143.7
73.29	187.6	0.3907	29.996	22.4	-2.480	2306.1699	10000	-6.087E-4	-7.049E-5	2882.7	2.8827E5	3.384E-3	0.5	1.5	89.996	224.85	150.1
76.65	192.7	0.3977	31.008	22.4	2.480	2438.9600	10000	6.087E-4	6.678E-5	3048.7	3.0487E5	3.384E-3	0.5	1.5	91.008	235.15	154.2
78.98	197.8	0.3992	31.996	22.4	-10.75	2565.4099	10000	-2.638E-3	-2.746E-4	3206.8	3.2068E5	3.384E-3	0.5	1.5	91.996	242.31	158.3
83.72	205.8	0.4067	33.012	22.4	-12.40	2774.0100	10000	-3.043E-3	-2.927E-4	3467.5	3.4675E5	3.383E-3	0.6	1.6	93.012	256.83	164.7
87.37	211.0	0.4141	33.996	22.4	-10.75	2913.0901	10000	-2.638E-3	-2.414E-4	3641.4	3.6414E5	3.384E-3	0.6	1.6	93.996	268.06	168.8
91.37	218.6	0.4180	35.008	22.4	-28.93	3127.9600	10000	-7.101E-3	-6.054E-4	3910.0	3.9100E5	3.384E-3	0.6	1.6	95.008	280.33	174.9
95.43	223.9	0.4262	36.012	22.4	-30.59	3280.9600	10000	-7.507E-3	-6.100E-4	4101.2	4.1012E5	3.384E-3	0.6	1.6	96.012	292.76	179.1
99.34	229.1	0.4336	36.996	22.4	-31.41	3431.1299	10000	-7.710E-3	-5.985E-4	4288.9	4.2889E5	3.383E-3	0.6	1.6	96.996	304.76	183.3
104.4	236.6	0.4410	38.000	22.4	-35.55	3659.2300	10000	-8.724E-3	-6.348E-4	4574.0	4.5740E5	3.384E-3	0.6	1.6	98.000	320.16	189.3
107.4	241.8	0.4442	39.012	22.4	-34.72	3826.7700	10000	-8.521E-3	-5.936E-4	4783.5	4.7835E5	3.384E-3	0.7	1.7	99.012	329.58	193.5
113.5	249.6	0.4548	39.996	22.4	-47.95	4068.9900	10000	-0.01177	-7.696E-4	5086.2	5.0862E5	3.384E-3	0.7	1.7	99.996	348.23	199.7
117.6	254.6	0.4617	40.996	22.4	-55.39	4233.2402	10000	-0.01359	-8.543E-4	5291.6	5.2916E5	3.384E-3	0.7	1.7	100.996	360.68	203.7
120.7	259.8	0.4644	42.000	22.4	-45.47	4409.7900	10000	-0.01116	-6.734E-4	5512.2	5.5122E5	3.383E-3	0.7	1.7	102.000	370.20	207.9
126.2	267.6	0.4716	42.996	22.4	-51.25	4674.9199	10000	-0.01258	-7.156E-4	5843.7	5.8437E5	3.384E-3	0.7	1.7	102.996	387.20	214.1
129.5	272.7	0.4751	43.996	22.4	-64.48	4851.7002	10000	-0.01583	-8.672E-4	6064.6	6.0646E5	3.384E-3	0.7	1.7	103.996	397.42	218.1
136.8	280.4	0.4881	44.996	22.4	-80.19	5129.2202	10000	-0.01968	-1.020E-3	6411.5	6.4115E5	3.383E-3	0.7	1.7	104.996	419.83	224.3
140.0	285.5	0.4902	45.996	22.4	-71.09	5321.7998	10000	-0.01745	-8.720E-4	6652.3	6.6523E5	3.384E-3	0.8	1.8	105.996	429.43	228.4
147.0	293.1	0.5014	46.996	22.4	-95.89	5602.5801	10000	-0.02354	-1.116E-3	7003.2	7.0032E5	3.383E-3	0.8	1.8	106.996	450.90	234.5
152.0	298.2	0.5097	47.996	22.4	-100.9	5799.1602	10000	-0.02475	-1.134E-3	7249.0	7.2490E5	3.384E-3	0.8	1.8	107.996	466.25	238.5
154.5	303.3	0.5095	48.996	22.4	-106.6	6000.7700	10000	-0.02617	-1.159E-3	7501.0	7.5010E5	3.383E-3	0.8	1.8	108.996	474.13	242.7
160.3	311.0	0.5154	49.996	22.4	-108.3	6302.7500	10000	-0.02658	-1.120E-3	7878.4	7.8784E5	3.383E-3	0.8	1.8	109.996	491.65	248.8
168.1	316.0	0.5318	51.012	22.4	-114.1	6510.8599	10000	-0.02800	-1.142E-3	8138.6	8.1386E5	3.383E-3	0.9	1.9	111.012	515.62	252.8
172.7	323.8	0.5332	51.996	22.4	-107.5	6832.4199	10000	-0.02638	-1.025E-3	8540.5	8.5405E5	3.384E-3	0.9	1.9	111.996	529.69	259.0
177.3	328.9	0.5390	52.996	22.4	-136.4	7050.1899	10000	-0.03348	-1.261E-3	8812.7	8.8127E5	3.384E-3	0.9	1.9	112.996	543.86	263.1
184.1	336.4	0.5472	54.012	22.4	-140.5	7374.8198	10000	-0.03449	-1.242E-3	9218.5	9.2185E5	3.383E-3	0.9	1.9	114.012	564.81	269.1
187.2	341.6	0.5480	54.996	22.4	-144.7	7601.8799	10000	-0.03551	-1.240E-3	9502.4	9.5024E5	3.384E-3	0.9	1.9	114.996	574.36	273.3
191.5	346.7	0.5524	55.992	22.4	-144.7	7828.7402	10000	-0.03551	-1.203E-3	9785.9	9.7859E5	3.384E-3	0.9	1.9	115.992	587.54	277.4
199.6	354.2	0.5636	57.012	22.4	-182.7	8169.1802	10000	-0.04484	-1.456E-3	10211	1.0211E6	3.383E-3	1.0	2.0	117.012	612.47	283.4
203.5	359.3	0.5662	58.012	22.4	-176.9	8408.7998	10000	-0.04342	-1.370E-3	10511	1.0511E6	3.383E-3	1.0	2.0	118.012	624.26	287.5
211.7	367.0	0.5768	58.996	22.4	-127.3	8768.1699	10000	-0.03125	-9.452E-4	10960	1.0960E6	3.384E-3	1.0	2.0	118.996	649.43	293.6
216.7	372.0	0.5825	59.992	22.4	-198.4	9010.5703	10000	-0.04869	-1.434E-3	11263	1.1263E6	3.384E-3	1.0	2.0	119.992	664.79	297.6

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

222.5	375.0	0.5933	0.99600	22.4	-205.0	315.4730	10000	-0.05032	-1.458E-3	394.34	39434	3.383E-3	0.0	2.0	121.996	682.53	300.0
219.1	375.0	0.5842	2.0000	22.4	-232.3	564.2650	10000	-0.05701	-1.652E-3	705.33	70533	3.384E-3	0.0	2.1	123.000	672.07	300.0
220.1	375.0	0.5869	2.9920	22.4	-191.0	815.5880	10000	-0.04687	-1.358E-3	1019.5	1.0195E5	3.384E-3	0.0	2.1	123.992	675.21	300.0
219.0	375.0	0.5839	3.9960	22.4	-210.8	1192.4700	10000	-0.05174	-1.499E-3	1490.6	1.4906E5	3.384E-3	0.1	2.1	124.996	671.80	300.0
220.5	375.0	0.5880	4.9920	22.4	-224.8	1444.0400	10000	-0.05519	-1.599E-3	1805.1	1.8051E5	3.383E-3	0.1	2.1	125.992	676.42	300.0
218.2	375.0	0.5820	5.9960	22.4	-193.4	1823.7400	10000	-0.04748	-1.376E-3	2279.7	2.2797E5	3.383E-3	0.1	2.1	126.996	669.56	300.0
219.8	375.0	0.5862	7.0040	22.4	-187.6	2072.2500	10000	-0.04606	-1.334E-3	2590.3	2.5903E5	3.384E-3	0.1	2.1	128.004	674.45	300.0
218.7	375.0	0.5833	7.9920	22.4	-224.0	2323.4600	10000	-0.05498	-1.593E-3	2904.3	2.9043E5	3.384E-3	0.1	2.1	128.992	671.08	300.0
219.5	375.0	0.5855	9.0000	22.4	-182.7	2700.5701	10000	-0.04484	-1.299E-3	3375.7	3.3757E5	3.384E-3	0.2	2.2	130.000	673.54	300.0
219.0	375.0	0.5840	9.9960	22.4	-176.1	2953.0901	10000	-0.04322	-1.252E-3	3691.4	3.6914E5	3.383E-3	0.2	2.2	130.996	671.86	300.0
219.2	375.0	0.5846	10.988	22.4	-141.4	3203.3000	10000	-0.03469	-1.005E-3	4004.1	4.0041E5	3.383E-3	0.2	2.2	131.988	672.62	300.0
219.5	375.0	0.5853	11.992	22.4	-199.2	3582.3301	10000	-0.04890	-1.417E-3	4477.9	4.4779E5	3.384E-3	0.2	2.2	132.992	673.35	300.0
218.4	375.0	0.5824	12.992	22.4	-210.8	3831.5601	10000	-0.05174	-1.499E-3	4789.5	4.7895E5	3.384E-3	0.2	2.2	133.992	670.00	300.0
219.8	375.0	0.5862	14.004	22.4	-144.7	4208.4399	10000	-0.03551	-1.029E-3	5260.6	5.2606E5	3.384E-3	0.2	2.3	135.004	674.36	300.0
219.0	375.0	0.5839	14.996	22.4	-176.9	4459.8301	10000	-0.04342	-1.258E-3	5574.8	5.5748E5	3.383E-3	0.2	2.3	135.996	671.77	300.0
217.9	375.0	0.5810	15.992	22.4	-159.5	4711.2100	10000	-0.03916	-1.135E-3	5889.0	5.8890E5	3.383E-3	0.3	2.3	136.992	668.38	300.0
218.6	375.0	0.5830	16.996	22.4	-205.8	5088.1899	10000	-0.05052	-1.464E-3	6360.2	6.3602E5	3.383E-3	0.3	2.3	137.996	670.78	300.0
222.5	375.0	0.5933	17.992	22.4	-184.3	5339.5498	10000	-0.04524	-1.311E-3	6674.4	6.6744E5	3.384E-3	0.3	2.3	138.992	682.58	300.0
222.7	375.0	0.5939	19.000	22.4	-201.7	5729.8999	10000	-0.04951	-1.434E-3	7162.4	7.1624E5	3.384E-3	0.3	2.3	140.000	683.23	300.0
220.6	375.0	0.5883	19.996	22.4	-161.2	5969.1201	10000	-0.03956	-1.146E-3	7461.4	7.4614E5	3.384E-3	0.3	2.3	140.996	676.80	300.0
221.3	375.0	0.5900	20.992	22.4	-154.6	6220.4702	10000	-0.03794	-1.099E-3	7775.6	7.7756E5	3.384E-3	0.3	2.4	141.992	678.81	300.0
221.9	375.0	0.5919	21.996	22.4	-182.7	6596.0898	10000	-0.04484	-1.299E-3	8245.1	8.2451E5	3.384E-3	0.4	2.4	142.996	680.90	300.0
220.1	375.0	0.5869	22.992	22.4	-189.3	6847.5601	10000	-0.04646	-1.346E-3	8559.5	8.5595E5	3.384E-3	0.4	2.4	143.992	675.22	300.0

